Volume 8 Issue 1
Feb.  2023
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Article Navigation >  Green Energy&Environment  > 2023  >  8(1): 183-193
Songlin Wang, Qiying Zhang, Chengxing Cui, Hongying Niu, Cailing Wu, Jianji Wang. Ionic liquids-SBA-15 hybrid catalysts for highly efficient and solvent-free synthesis of diphenyl carbonate. Green Energy&Environment, 2023, 8(1): 183-193. doi: 10.1016/j.gee.2021.02.010
Citation: Songlin Wang, Qiying Zhang, Chengxing Cui, Hongying Niu, Cailing Wu, Jianji Wang. Ionic liquids-SBA-15 hybrid catalysts for highly efficient and solvent-free synthesis of diphenyl carbonate. Green Energy&Environment, 2023, 8(1): 183-193. doi: 10.1016/j.gee.2021.02.010
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Ionic liquids-SBA-15 hybrid catalysts for highly efficient and solvent-free synthesis of diphenyl carbonate

doi: 10.1016/j.gee.2021.02.010

  • a. Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, 453007, China;

  • b. School of Chemistry and Chemical Engineering, Henan Institute of Science and Technology, Xinxiang, 453003, China

Funds:

Technology Innovation Talents in Universities of Henan Province (23HASTIT014), Postgraduate Education Reform and Quality Improvement Project of Henan Province (YJS2022KC22), Project funded by China Postdoctoral Science Foundation (No. 2018M632782), Project funded by Postdoctoral Research Grant in Henan Province (No. 001802030), Key Project of Science and Technology Program of Henan Province (No. 222102230109, 212102310330 and 182102210050), and the Science Research Start-up Fund of Henan Institute of Science and Technology (No. 2015031).

We gratefully acknowledge the financial support from the National Natural Science Foundation of China (No. 21808048 and U1704251), Training Plan for University's Young Backbone Teachers of Henan Province (2021GGJS121), Program for Science &

  • Received date 06 November 2020, Accepted date 22 February 2021, RevRecd date 01 January 2021, Publish date 24 February 2021,
    Abstract
  • Diphenyl carbonate (DPC) is one of the versatile carbonates, and is often used for the production of polycarbonates. In recent years, the catalytic synthesis of DPC has become an important topic but the development of a highly active metal-free catalyst is a great challenge. Herein, a series of ionic liquids-SBA-15 hybrid catalysts with different functional groups have been developed for the synthesis of DPC under solvent-free condition, which are effective and clean instead of the metal-containing catalysts. It is found that in the presence of [SBA-15-IL-OH]Br catalyst, methyl phenyl carbonate (MPC) conversion of 80.5% along with 99.6% DPC selectivity is achieved, the TOF value is thrice higher than the best value reported by using transition metal-based catalysts. Moreover, the catalyst displays remarkable stability and recyclability. This work provides a new idea to design and prepare eco-friendly catalysts in a broad range of applications for the green synthesis of carbonates.

     

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