Volume 9 Issue 4
Apr.  2024
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A.K.K. Vikla, K. Koichumanova, Songbo He, K. Seshan. Aqueous-phase reforming of hydroxyacetone solution to bio-based H2 over supported Pt catalysts. Green Energy&Environment, 2024, 9(4): 777-788. doi: 10.1016/j.gee.2022.09.002
Citation: A.K.K. Vikla, K. Koichumanova, Songbo He, K. Seshan. Aqueous-phase reforming of hydroxyacetone solution to bio-based H2 over supported Pt catalysts. Green Energy&Environment, 2024, 9(4): 777-788. doi: 10.1016/j.gee.2022.09.002
shu

Aqueous-phase reforming of hydroxyacetone solution to bio-based H2 over supported Pt catalysts

doi: 10.1016/j.gee.2022.09.002

  • a. Joint International Research Laboratory of Circular Carbon, Nanjing Tech University, Nanjing, 211816, China;

  • b. Faculty of Science and Technology, University of Twente, 7500 AE Enschede, The Netherlands;

  • c. CoRe Pro, 9723 BL Groningen, The Netherlands

Funds:

Financial support from European Union Seventh Framework Programme (FP7/2007–2013 project SusFuelCat, grant No. 310490) is acknowledged. The authors would like to acknowledge Ing. B. Geerdink for his technical support when carrying out the APR experiments and for setting up of TPO equipment. Ing. Benno Knaken is thanked for his expertise in maintaining the high-pressure reactors. Mrs. K. Altena-Schildkamp is thanked for BET and CO chemisorption measurements. Prof. Dr. L. Lefferts is thanked for preliminary discussions. Dr. Irina Simakova from Boreskov Institute of Catalysis is thanked for providing the Sibunit support and also for her assistance with XRF measurements.

  • Received date 17 April 2022, Accepted date 02 September 2022, RevRecd date 30 August 2022, Publish date 08 September 2022,
    Abstract
  • Aqueous-phase reforming (APR) is an attractive process to produce bio-based hydrogen from waste biomass streams, during which the catalyst stability is often challenged due to the harsh reaction conditions. In this work, three Pt-based catalysts supported on C, AlO(OH), and ZrO2 were investigated for the APR of hydroxyacetone solution in a fixed bed reactor at 225 ℃ and 35 bar. Among them, the Pt/C catalyst showed the highest turnover frequency for H2 production (TOF of 8.9 mol molPt-1 min-1) and the longest catalyst stability. Over the AlO(OH) and ZrO2 supported Pt catalysts, the side reactions consuming H2, formation of coke, and Pt sintering result in a low H2 production and the fast catalyst deactivation. The proposed reaction pathways suggest that a promising APR catalyst should reform all oxygenates in the aqueous phase, minimize the hydrogenation of the oxygenates, maximize the WGS reaction, and inhibit the condensation and coking reactions for maximizing the hydrogen yield and a stable catalytic performance.

     

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