Volume 7 Issue 6
Dec.  2022
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Article Navigation >  Green Energy&Environment  > 2022  >  7(6): 1281-1288
Mingzhao Xu, Lifei Liu, Jianling Zhang, Fanyu Zhang, Gang Chen, Qiang Wan, Yufei Sha, Xiuyan Cheng, Zhuizhui Su. Ferric acetylacetonate/covalent organic framework composite for high performance photocatalytic oxidation. Green Energy&Environment, 2022, 7(6): 1281-1288. doi: 10.1016/j.gee.2021.02.001
Citation: Mingzhao Xu, Lifei Liu, Jianling Zhang, Fanyu Zhang, Gang Chen, Qiang Wan, Yufei Sha, Xiuyan Cheng, Zhuizhui Su. Ferric acetylacetonate/covalent organic framework composite for high performance photocatalytic oxidation. Green Energy&Environment, 2022, 7(6): 1281-1288. doi: 10.1016/j.gee.2021.02.001
shu

Ferric acetylacetonate/covalent organic framework composite for high performance photocatalytic oxidation

doi: 10.1016/j.gee.2021.02.001

  • a. Beijing National Laboratory for Molecular Sciences, CAS Key Laboratory of Colloid and Interface and Thermodynamics, CAS Research/Education Center for Excellence in Molecular Sciences, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100190, China;

  • b. School of Chemistry and Chemical Engineering, University of Chinese Academy of Sciences, Beijing, 100049, China;

  • c. School of Chemical Sciences, University of Chinese Academy of Sciences, Physical Science Laboratory, Huairou National Comprehensive, Science Center, Beijing, 100190, China

Funds:

The authors thank the financial supports from National Natural Science Foundation of China (21525316, 21673254), Ministry of Science and Technology of China (2017YFA0403003), Chinese Academy of Sciences (QYZDY-SSW-SLH013) and Beijing Municipal Science & Technology Commission (Z191100007219009).

  • Received date 29 November 2020, Accepted date 01 February 2021, RevRecd date 31 January 2021, Publish date 31 December 2022,
    Abstract
  • Ferric acetylacetonate/covalent organic framework (Fe(acac)3/COF) composite was synthesized by interfacial polymerization method at room temperature. The crystal structure, morphology and porosity property of the composite were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope and nitrogen adsorption. The interaction between Fe(acac)3 and COF was investigated by Fourier transform infrared spectra and X-ray photoelectron spectroscopy. The Fe(acac)3/COF composite was used as a photocatalyst for the oxidation of benzyl alcohol under mild conditions. It exhibits high activity and selectivity for the reaction, of which the mechanism was investigated by determining its photoelectric properties. The Fe(acac)3/COF catalyst developed in this work has application potential in other photocatalytic reactions.

     

    • • A ferric acetylacetonate/covalent organic framework composite was synthesized using interfacial polymerization method. • The composite exhibits excellent light absorbance and transformation of photogenerated electron–hole pairs. • The composite shows high catalytic performance for the selective oxidation of benzyl alcohol under mild conditions.
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