Volume 7 Issue 6
Dec.  2022
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Article Navigation >  Green Energy&Environment  > 2022  >  7(6): 1310-1317
Zengyong Li, Yiming Huang, Xiao Chi, Di Li, Linxin Zhong, Xuehui Li, Chuanfu Liu, Xinwen Peng. Biomass-based N doped carbon as metal-free catalyst for selective oxidation of D-xylose into D-xylonic acid. Green Energy&Environment, 2022, 7(6): 1310-1317. doi: 10.1016/j.gee.2021.01.004
Citation: Zengyong Li, Yiming Huang, Xiao Chi, Di Li, Linxin Zhong, Xuehui Li, Chuanfu Liu, Xinwen Peng. Biomass-based N doped carbon as metal-free catalyst for selective oxidation of D-xylose into D-xylonic acid. Green Energy&Environment, 2022, 7(6): 1310-1317. doi: 10.1016/j.gee.2021.01.004
shu

Biomass-based N doped carbon as metal-free catalyst for selective oxidation of D-xylose into D-xylonic acid

doi: 10.1016/j.gee.2021.01.004

  • a. State Key Laboratory of Pulp and Paper Engineering, South China University of Technology, Guangzhou, 510640, China;

  • b. School of Chemistry and Chemical Engineering, South China University of Technology, Guangzhou, 510640, China

Funds:

This work was supported by Fundamental Research Funds for the Central Universities (2019PY13), National Program for Support of Top-notch Young Professionals, Science and Technology Basic Resources Investigation Program of China (2019FY100903), National Natural Science Foundation of China (31971614), Guangdong Natural Science Funds for Distinguished Young Scholar (2016A030306027), Guangdong Natural Science Funds (2017A030313130), Guangzhou science and technology funds (201904010078), State Key Lab of Pulp and Paper Engineering (2020C03), and China Postdoctoral Science Foundation Grant (2019T120725, 2019M652882).

  • Received date 30 September 2020, Accepted date 06 January 2021, RevRecd date 22 December 2020, Publish date 31 December 2022,
    Abstract
  • Rational design and facile preparation of low-cost and efficient catalysts for the selective converting of biomass-derived monosaccharides into high value-added chemicals is highly demanded, yet challenging. Herein, we first demonstrate a N doped defect-rich carbon (NC-800-5) as metal-free catalyst for the selective oxidation of D-xylose into D-xylonic acid in alkaline aqueous solution at 100°C for 30 min, with 57.4% yield. The doped graphitic N is found to be the active site and hydroxyl ion participating in the oxidation of D-xylose. Hydroxyl ion and D-xylose first adsorb on NC-800-5 surface, and the aldehyde group of D-xylose is catalyzed to form germinal diols ion. Then, C–H bond break to yield carboxylic group. Furthermore, NC-800-5 catalyst shows high stability in recycled test.

     

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