Volume 7 Issue 5
Oct.  2022
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Article Navigation >  Green Energy&Environment  > 2022  >  7(5): 975-982
Haoyuan Chi, Jingwen Dong, Tian Li, Sha Bai, Ling Tan, Jikang Wang, Tianyang Shen, Guihao Liu, Lihong Liu, Luyi Sun, Yufei Zhao, Yu-Fei Song. Scaled-up synthesis of defect-rich layered double hydroxide monolayers without organic species for efficient oxygen evolution reaction. Green Energy&Environment, 2022, 7(5): 975-982. doi: 10.1016/j.gee.2020.12.013
Citation: Haoyuan Chi, Jingwen Dong, Tian Li, Sha Bai, Ling Tan, Jikang Wang, Tianyang Shen, Guihao Liu, Lihong Liu, Luyi Sun, Yufei Zhao, Yu-Fei Song. Scaled-up synthesis of defect-rich layered double hydroxide monolayers without organic species for efficient oxygen evolution reaction. Green Energy&Environment, 2022, 7(5): 975-982. doi: 10.1016/j.gee.2020.12.013
shu

Scaled-up synthesis of defect-rich layered double hydroxide monolayers without organic species for efficient oxygen evolution reaction

doi: 10.1016/j.gee.2020.12.013

  • a State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, China;

  • b College of Chemistry, Key Laboratory of Theoretical & Computational Photochemistry of Ministry of Education, Beijing Normal University, Beijing, 100875, China;

  • c Polymer Program, Institute of Materials Science and Department of Chemical & Biomolecular Engineering, University of Connecticut, Storrs, Connecticut, 06269, USA;

  • d Beijing Advanced Innovation Center for Soft Matter Science and Engineering, Beijing University of Chemical Technology, Beijing, 100029, China

Funds:

This research was supported by the National Nature Science Foundation of China (U1707603, 21878008, 21625101, U1507102, 21922801), the Beijing Natural Science Foundation (2182047, 2202036) and the Fundamental Research Funds for the Central Universities (XK1802-6, XK1902, 12060093063, 2312018RC07). The XAFS experiments were conducted in 1W1B beamline of Beijing Synchrotron Radiation Facility (BSRF).

  • Received date 01 October 2020, Accepted date 13 December 2020, RevRecd date 12 December 2020, Publish date 21 December 2020,
    Abstract
  • The scaled-up synthesis of organic-free monolayer nanomaterials is highly desirable, especially in obtaining green energy by electrocatalysis. In this study, a method for the scaled-up synthesis of the series of monolayer layered double hydroxides (LDHs) without the addition of organic solvents is reported via the separate nucleation and aging steps process. The resulting monolayer LDHs with the thicknesses of less than 1 nm showed a narrow thickness distribution. X-ray absorption fine-structure revealed that monolayer NiFe-LDH nanosheets have a number of oxygen and metal vacancies defects. As a practical application, monolayer NiFe-LDH nanosheets containing defects showed an enhanced electrocatalytic water oxidation activity compared with that of bulk NiFe-LDH. Density functional theory calculations uncovered that excellent catalytic activity is attributed to vacancies defects. The proposed method is an economical and universally applicable strategy for the scaled-up production of monolayer LDHs.

     

    • These authors contributed equally to this work.
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